Reconstruction of surface topographies by scanning electron microscopy for application in fracture research

نویسندگان

  • J. Stampfl
  • S. Scherer
  • M. Gruber
  • O. Kolednik
چکیده

Stereoscopic scanning electron micrographs can be used to reconstruct the microscopic topography of material surfaces. By applying a system for automatic image processing we can obtain Digital Elevation Models (DEMs) of the investigated surface. These DEMs are used to measure the degree of deformation on metallic fracture surfaces. By modelling the deformation the amount of plastic energy that is necessary to shape the microductile fracture surface can be calculated. These values are compared with experimentally obtained results. PACS: 07.80; 42.30; 62.00 The usability of a certain material in a mechanically loaded structure is limited by its strength. The higher the yield strength the larger are the possible loads. A problem arises when there exist precracks in the structure, e.g. caused by fatigue or corrosion. In this case the stresses concentrate at sharp notches (like cracks are) and they can become large enough to cause final failure although the average stress is below the yield stress. Especially, materials with high yield strengths have the tendency to break at low stress intensities since they are brittle and cannot diminish the stress intensities by blunting of the sharp crack tip. That is why, in addition to the strength, a second mechanical parameter (the fracture toughness) must be introduced to estimate the mechanical reliability of a structure. One established parameter for the determination of fracture toughness is the energy dissipation rate D [1, 2] which is related to the amount of plastic energy that is necessary to propagate a crack. Three mechanisms contribute to the dissipation of energy during the crack extension: A certain fraction of the overall dissipated plastic energy is spent for the lateral necking of the specimen, another fraction is spent for deformations within the plastic zone outside the process zone. The third mechanism which dissipates energy is the formation of voids in the process zone. This energy term will further be called void energy. When the voids in the process zone grow and coalesce, the crack length increases. The surface topography is reconstructed by analyzing stereoscopic Scanning Electron Microscope (SEM) images. The technique [3—8] allows the reconstruction of a 3D-object by measuring the parallaxes in two stereo images. By using a system for image processing [9, 10] we can automatically generate DEMs consisting of about 10 000 points. The aim of this work is to estimate the amount of the void energy from analyzing the plastic deformations that led to the final fracture surface topography. Similar estimations were already done in earlier works [11, 12] by modelling the surface topography with a parabolic or ellipsoidal dimple profile. In this work, due to the use of automatic image processing, the real surface shape can be taken into account for the calculation of the deformation energy and no assumptions about the surface profile have to be made.

برای دانلود رایگان متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Application of Scanning Electron and Atomic Force Mode Microscopy on inscription from Proto-Elamite period in Tappeh Sofalin

The study of cultural heritage artifacts and the research of a protection and restoration intervention create with - and are often limited to - a complete characterization of their surface. This is not only factual for museum objects, but also for archaeological artifacts, because the object as it was discovered may contain precious unknown information that could be lost by too much aggressive ...

متن کامل

Wavelength-dependent roughness: a quantitative approach to characterizing the topography of rough titanium surfaces.

Topographies of grit-blasted, etched, grit-blasted and etched, and microfabricated and etched surfaces of commercially pure titanium have been investigated. Such surface topographies vary across the scale range of interest for dental implants, extending from nanometers to millimeters. The complete characterization of topography requires the use of complementary methods. This study compared the ...

متن کامل

Microstructure and Mechanical Properties of the Friction Welded Joint between X53CrMnNiN219 and X45CrSi93 Stainless Steel

Dissimilar metals friction welding of austenitic–martensitic stainless steels is commonly used in order to manufacture engine valves in the automobile industry. In this study, X53CrMnNiN219 (austenitic stainless steel) and X45CrSi93 (martensitic stainless steel) valve steel rods were welded by friction welding process. The welded joint was then heat treated at 760 0C for 60 min. Mechanical prop...

متن کامل

Correlative fractography: combining scanning electron microscopy and light microscopes for qualitative and quantitative analysis of fracture surfaces.

Correlative fractography is a new expression proposed here to describe a new method for the association between scanning electron microscopy (SEM) and light microscopy (LM) for the qualitative and quantitative analysis of fracture surfaces. This article presents a new method involving the fusion of one elevation map obtained by extended depth from focus reconstruction from LM with exactly the s...

متن کامل

High-performance starch-modified graphene oxide/epoxy nanocomposite coatings: A glimpse at cure kinetics and fracture behavior

Epoxy is a versatile resin used in different fields such as coatings, colors, colorants, and composites. Adding nano-scale fillers/additives to the epoxy has valued epoxy coatings for engineering applications, and opened the time of advanced epoxy-based nanocomposite coatings. In the present work, graphene oxide GO was chemically functionalized with starch, as a natural polymer, and added to th...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

عنوان ژورنال:

دوره   شماره 

صفحات  -

تاریخ انتشار 1996